Fiber Reinforced Plastics/Composites ›› 2010, Vol. 210 ›› Issue (1): 67-69.
• EQUIPMENT PROCESS • Previous Articles Next Articles
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Abstract:
To optimize the processing technology for pentaerythrityl tetrabromide with yield ratio as a marker,with the method of orthogonal experimental design,the paper investigates the influencing factors such as reaction time,reaction temperature and the content of catalyst. The result shows that the optimum condition of processing technology is reactive for 14 hours,with the temperature of 140~150℃, and the content of catalyst is 1.5g. The reaction time has significant effect on the yield ratio.
Key words: pentaerythrityl tetrabromide, orthogonal design, processing technology, yield ratio
CLC Number:
TQ222.2+15
Chen, S. J., Z. J. J., Meng, Y.. OPTIMIZATION OF PROCESSING TECHNOLOGY FOR PENTAERYTHRITYL TETRABROMIDE WITH ORTHOGONAL DESIGN[J]. Fiber Reinforced Plastics/Composites, 2010, 210(1): 67-69.
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[1] Herzog H L. Pentaerythrityl Tetrabromide [M].In. Org. Synth., Coll Vol II. New York: John Willey and Sons, 1943:476478. [2] Edwin R, Buchman A C. Pentaerythrityl sulfonates [P].USP 2703808, 1951. [3] 魏运洋,邵云.季戊四胺的改良合成[J].含能材料,2002, 2 (10): 4951. [4] 武志胜.工艺条件对ZrO2粒度的影响[J].纤维复合材料,2005, 4:3334. [5] 姜同川.正交试验设计[M].山东科学技术出版社,1985. [6] 琚晓晖,齐鲁.有机硅改性三聚氰胺甲醛树脂的性能[J],纤维复合材料,2006, 12(1):1215. [7] 王海东,王均,杨小利.高光表面SMC的研究[J].玻璃钢/复合材料,2005,(3):3436. [8] 杨宇,刁梦雪,周俐宏等.煤炭生物脱硫正交实验研究[J].生态环境, 2008, 17(2):459465. [9] 段华军,王均,杨小利.低粘度环氧树脂固化体系研究[J].玻璃钢/复合材料, 2004, (1):3234. [10] 梁荣宁,叶庆国.重氮化水解法合成间甲酚的工艺研究[J].化工中间体, 2008, (3):1416. [11] 李建权,颜世涛.聚合物改性纤维增强水泥复合材料的耐水性研究[J].玻璃钢/复合材料, 2003, (2):2223. [12] 吕龙,郭成金.正交设计法探讨茯苓原生质体的最佳制备条件[J].天津师范大学学报(自然科学版),2007, 37(3):3135.